The Annals of “Dunarea de Jos” University of Galati. Fascicle IX, Metallurgy and Materials Science https://gup.ugal.ro/ugaljournals/index.php/mms <p style="margin: 0cm; margin-bottom: .0001pt;"><strong>DOI:</strong> <a href="https://doi.org/10.35219/mms" target="_blank" rel="noopener">https://doi.org/10.35219/mms</a></p> <p style="margin: 0cm; margin-bottom: .0001pt;"><strong>CNCSIS CODE:</strong> 215,&nbsp; B+ Category</p> <p style="margin: 0cm; margin-bottom: .0001pt;"><strong>ISSN</strong> 2668-4748; <strong>E-ISSN</strong> 2668-4756</p> <p style="margin: 0cm; margin-bottom: .0001pt;"><strong>Frequency:</strong> quarterly (2010- ), biannual (2005-2009)</p> <p style="margin: 0cm; margin-bottom: .0001pt;"><strong>Subjects covered:</strong>&nbsp;metallurgy and materials science,&nbsp;environment, chemistry, mechanics, energy</p> <p style="margin: 0cm; margin-bottom: .0001pt;"><strong>Contact:</strong> marius.bodor@ugal.ro</p> "Dunarea de Jos" University of Galati en-US The Annals of “Dunarea de Jos” University of Galati. Fascicle IX, Metallurgy and Materials Science 2668-4748 Deep Learning-Based Camouflage Detection for Anti-Personnel Mine Identification in Natural Environments https://gup.ugal.ro/ugaljournals/index.php/mms/article/view/10120 <p>The detection of anti-personnel mines in natural environments remains a&nbsp;critical humanitarian and technological challenge due to the high visual similarity&nbsp;between explosive devices and their surrounding backgrounds. This study presents&nbsp;a deep learning-based camouflage detection framework for the identification and&nbsp;segmentation of PFM-1 anti-personnel mine surrogates embedded in visually&nbsp;homogeneous outdoor scenes. The proposed approach employs a Deep Camouflage&nbsp;Detection Network (DCDN) designed to extract multi-scale contextual features and&nbsp;enhance boundary sensitivity under low-contrast conditions. A dedicated dataset&nbsp;was constructed using 3D-printed PFM-1 surrogates positioned in vegetated&nbsp;environments under varying illumination conditions, viewing angles, occlusion&nbsp;levels, and object scales. The network architecture integrates a pretrained&nbsp;convolutional backbone, multi-scale feature aggregation modules, and a&nbsp; composite&nbsp;loss function (consisting of Binary Cross-Entropy and Dice loss) to address class&nbsp;imbalance and weak edge contrast.<br>Experimental evaluation on an independent test set demonstrates robust&nbsp;segmentation performance, achieving a mean Intersection over Union (IoU) of&nbsp;91.8% and a Dice coefficient of 95.7%. Precision and recall values of 96.3% and&nbsp;94.9%, respectively, confirm a balanced detection capability with limited false&nbsp;positives. Stratified analysis indicates stable performance under illumination&nbsp;variability and partial occlusion, while ablation studies highlight the importance of&nbsp;multi-scale aggregation and region-aware loss optimization. The results confirm&nbsp;that deep camouflage-aware segmentation architectures provide reliable detection&nbsp;of low-contrast objects in complex natural environments.</p> <p><a href="http://creativecommons.org/licenses/by-nc/4.0/"><img src="https://i.creativecommons.org/l/by-nc/4.0/88x31.png" alt="Creative Commons License"></a></p> Florin-Bogdan MARIN Mihaela MARIN ##submission.copyrightStatement## 2026-06-15 2026-06-15 49 2 5 9 10.35219/mms.2026.2.01 Fracture Behavior of Dissimilar Resistance Spot Welded Overlap Joint https://gup.ugal.ro/ugaljournals/index.php/mms/article/view/10121 <p>The resistance spot welding process is also used for the welding of dissimilar&nbsp;materials. A dissimilar join is formed by two sheets: a 1.0 mm thick sheet of lowalloy&nbsp;carbon steel and a 1.5 mm thick sheet of aluminium alloy 6061 T6. In this&nbsp;study, the effects of welding current and nugget diameter are investigated. Welding&nbsp;times and welding force are kept constant. Tensile shear tests were applied in order&nbsp;to determine the strength parameters of the dissimilar joint. The experimental&nbsp;results show that an increase in the welding current increases the tensile shear&nbsp;stress and the weld nugget diameter. This study used a fracture mechanics-based&nbsp;approach, to investigate the influence of resistance spot welding parameters on the&nbsp;critical stress intensity factor. The results show that the critical stress intensity&nbsp;factor is maximal for a welding current equal to 16 kA. Also, the maximum tensile&nbsp;shear strength is achieved at an 8 mm nugget diameter, which is influenced by an&nbsp;increase in the welding current.</p> <p><a href="http://creativecommons.org/licenses/by-nc/4.0/"><img src="https://i.creativecommons.org/l/by-nc/4.0/88x31.png" alt="Creative Commons License"></a></p> Abdelkader BENYOUCEF Mustapha BENACHOUR Nadjia BENACHOUR Fatima Zohra SERIARI ##submission.copyrightStatement## 2026-06-15 2026-06-15 49 2 10 15 10.35219/mms.2026.2.02 Simulation of the Mechanical Stress Behavior in the Case of the Damascus Steel After Heat Treatments for Improvement https://gup.ugal.ro/ugaljournals/index.php/mms/article/view/10122 <p>The paper aims to study the behavior of Damascus steel at a maximum&nbsp;admissible load with a force of 250 N. Previous studies considered lower loading&nbsp;force values that did not produce cracks in the material. The processing of the&nbsp;samples and laboratory tests were carried out on specimens of Damascus steel&nbsp;obtained in the laboratory. The applied treatments were hardening and tempering&nbsp;to improve the material’s properties. The processing of the results and the&nbsp;simulations were carried out using Autodesk Inventor Professional 2023.</p> <p><a href="http://creativecommons.org/licenses/by-nc/4.0/"><img src="https://i.creativecommons.org/l/by-nc/4.0/88x31.png" alt="Creative Commons License"></a></p> Carmen-Penelopi PAPADATU ##submission.copyrightStatement## 2026-06-15 2026-06-15 49 2 16 21 10.35219/mms.2026.2.03 Assessment of Pollutant Load and Potential Impact of the Snowpack in Brăila Municipality https://gup.ugal.ro/ugaljournals/index.php/mms/article/view/10123 <p>Urban snowpack represents a highly effective matrix for monitoring&nbsp;atmospheric deposition, as it has the capacity to accumulate pollutants originating&nbsp;from anthropogenic activities during the cold season. The present study aims to&nbsp;assess the contamination levels of snow collected from different functional areas of&nbsp;the Brăila municipality, as well as to estimate the potential impact of pollutants on&nbsp;soil and surface waters during the melting period. Snow samples were collected&nbsp;from areas characterized by intense road traffic, residential zones, industrial&nbsp;sectors, and green spaces, in order to highlight the spatial variability of contaminants. Laboratory analyses included the determination of physicochemical&nbsp;parameters (pH, total dissolved solids, and electrical conductivity), major ionic&nbsp;species (Cl⁻, SO₄²⁻, NO₃⁻, NH₄⁺, Ca²⁺, Mg²⁺), and selected heavy metals (Pb, Cd, Fe),&nbsp;which are relevant indicators for identifying sources of urban pollution. The&nbsp;assessment of pollution levels was carried out using specific indices, such as the&nbsp;contamination factor and the pollution load index. The obtained results highlight&nbsp;the influence of anthropogenic activities on the chemical composition of urban&nbsp;snow and emphasize its role as a vector for pollutant transfer to soils and drainage&nbsp;systems during snowmelt. Ultimately, this study contributes to a better&nbsp;understanding of seasonal urban pollution processes and provides a scientific basis&nbsp;for the development of sustainable environmental management measures.</p> <p><a href="http://creativecommons.org/licenses/by-nc/4.0/"><img src="https://i.creativecommons.org/l/by-nc/4.0/88x31.png" alt="Creative Commons License"></a></p> Nicoleta CIOBOTARU ##submission.copyrightStatement## 2026-06-15 2026-06-15 49 2 22 28 10.35219/mms.2026.2.04 Failure Case Study Series Part Two: Failure Analysis of Roller Guides in a Wire Rod Rolling Mill https://gup.ugal.ro/ugaljournals/index.php/mms/article/view/10124 <p>The paper aims to present the root cause of failure of roller guides from the&nbsp;wire rod and coil rolling mill during normal operation. A comprehensive failure&nbsp;investigation was conducted following standard metallurgical procedures,&nbsp;including visual inspection, hardness testing, chemical analysis, optical&nbsp;microscopy, stereomicroscopy, scanning electron microscopy (SEM–EDS)&nbsp;characterization, and inclusion rating according to ASTM E45. The investigation&nbsp;concludes that the primary root cause of failure was the use of D3 tool steel, which&nbsp;is unsuitable for components subjected to severe thermal cycling, resulting in&nbsp;progressive thermal fatigue damage and eventual catastrophic fracture. Moreover,&nbsp;the election of D2 or other Mo-V alloyed hot‑work tool steels, combined with&nbsp;appropriate surface hardening, is recommended to enhance service life under rolling mill operating conditions.</p> <p><a href="http://creativecommons.org/licenses/by-nc/4.0/"><img src="https://i.creativecommons.org/l/by-nc/4.0/88x31.png" alt="Creative Commons License"></a></p> Liviu GURĂU Florin MARIN Mihaela MARIN Cristian ȘTEFĂNESCU Gheorghe GURĂU ##submission.copyrightStatement## 2026-06-15 2026-06-15 49 2 29 38 10.35219/mms.2026.2.05 Failure Case Study Series Part Three: Investigation of Wear and Failure Mechanisms in Heavy-Duty Gear Coupling https://gup.ugal.ro/ugaljournals/index.php/mms/article/view/10125 <p>This paper investigates the failure mechanisms of the gear teeth in a heavyduty&nbsp;coupling, emphasizing the combined effects of mechanical loading,&nbsp;metallurgical microstructure, and tribological wear mechanisms.<br>Detailed characterization using optical microscopy (OM), scanning electron&nbsp;microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), and both chemical&nbsp;and mechanical testing identified pronounced wear and progressive degradation of the coupling sleeve, largely driven by operational misalignments and external&nbsp;contamination, such as mill cobbles. The analysis underscores the critical&nbsp;importance of precise material compatibility, a controlled hardness differential,&nbsp;and manufacturing accuracy in mitigating localized stress concentrations and wear.&nbsp;The findings highlight that abnormal wear progression results from a complex&nbsp;interaction among load redistribution owing to misalignment, tribological&nbsp;deterioration, manufacturing tolerances, and dynamic rotor–coupling interactions.&nbsp;Recommendations focus on optimizing design parameters, manufacturing&nbsp;processes, and operational routines to enhance the reliability, durability, and safety&nbsp;of high-torque coupling systems in harsh industrial environments.</p> <p><a href="http://creativecommons.org/licenses/by-nc/4.0/"><img src="https://i.creativecommons.org/l/by-nc/4.0/88x31.png" alt="Creative Commons License"></a></p> Liviu GURĂU Florin MARIN Mihaela MARIN Cristian ȘTEFĂNESCU Gheorghe GURĂU ##submission.copyrightStatement## 2026-06-15 2026-06-15 49 2 39 46 10.35219/mms.2026.2.06 Failure Case Study Series Part Four: Investigation of the Failure Mechanism of the Connecting Rod in an Industrial Oxygen Compressor https://gup.ugal.ro/ugaljournals/index.php/mms/article/view/10126 <p>This investigation addresses the catastrophic fracture of a connecting rod in&nbsp;an oxygen compressor unit during steady‑state operation. Owing to its function in&nbsp;transmitting cyclic compressive and tensile loads between the crankshaft and the&nbsp;piston, the connecting rod it’s a critical structural element.<br>The assessment employed a systematic multi‑technique protocol. Macroscopic&nbsp;fractography was used to document crack morphology, fracture‑surface&nbsp;topography, and subsidiary failure‑related surface markers. Representative&nbsp;specimens were preserved for laboratory evaluation. Material conformance was&nbsp;verified through chemical composition analysis and hardness measurements&nbsp;benchmarked against applicable standards. The internal structure, including phase&nbsp;distribution, cleanliness, inclusion content, and thermal‑processing quality, was&nbsp;examined using optical metallography (OM). High‑resolution scanning electron&nbsp;microscopy (SEM) combined with energy‑dispersive spectroscopy (EDS) enabled&nbsp;the identification of crack‑initiation sites, fracture mechanisms, and local&nbsp;compositional anomalies.</p> <p><a href="http://creativecommons.org/licenses/by-nc/4.0/"><img src="https://i.creativecommons.org/l/by-nc/4.0/88x31.png" alt="Creative Commons License"></a></p> Liviu GURĂU Florin MARIN Mihaela MARIN Cristian ȘTEFĂNESCU Gheorghe GURĂU ##submission.copyrightStatement## 2026-06-15 2026-06-15 49 2 47 55 10.35219/mms.2026.2.07 Functionalized Plasmonic Nanoparticles: Synthesis, Surface Engineering and Emerging Biomedical Applications https://gup.ugal.ro/ugaljournals/index.php/mms/article/view/10127 <p>Functionalized plasmonic nanoparticles have attracted significant attention in&nbsp;biomedical research due to their unique optical properties, high surface reactivity,&nbsp;and versatile surface chemistry. In this study, gold nanoparticles (AuNPs) were&nbsp;synthesized via the Turkevich citrate reduction method and subsequently&nbsp;functionalized using (3-glycidyloxypropyl) trimethoxysilane (GPTMS) to enhance&nbsp;their stability and surface reactivity. The synthesized and functionalized&nbsp;nanoparticles were comprehensively characterized using multiple analytical&nbsp;techniques. Morphological features and particle size distribution were investigated&nbsp;by transmission electron microscopy (TEM) and scanning electron microscopy&nbsp;(SEM), while elemental composition was confirmed by energy-dispersive X-ray&nbsp;spectroscopy (EDS). The crystalline structure was analysed using X-ray diffraction&nbsp;(XRD), and the average crystallite size was estimated using the Scherrer equation.&nbsp;Fourier-transform infrared spectroscopy (FTIR) was employed to identify surface&nbsp;functional groups and confirm successful GPTMS functionalization. Additionally,&nbsp;UV–Vis spectrophotometry was used to evaluate the optical properties of the&nbsp;nanoparticles and to assess their localized surface plasmon resonance (LSPR)&nbsp;behavior. The results demonstrate that the functionalized AuNPs exhibit stable&nbsp;colloidal properties, controlled morphology, and modified optical responses due to surface engineering. The presence of additional absorption features in the UV&nbsp;region highlights the influence of GPTMS on the interfacial environment of the&nbsp;nanoparticles. The obtained results underscore the potential of GPTMSfunctionalized gold nanoparticles for applications in nanomedicine, including&nbsp;biosensing, drug delivery, and optical bioimaging.</p> <p><a href="http://creativecommons.org/licenses/by-nc/4.0/"><img src="https://i.creativecommons.org/l/by-nc/4.0/88x31.png" alt="Creative Commons License"></a></p> Mariana BUȘILĂ ##submission.copyrightStatement## 2026-06-15 2026-06-15 49 2 56 62 10.35219/mms.2026.2.08